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  • Originally posted by kedigen
    Beyond Biodiesel
    before 2kg, 6 kg and 30 kg prototoip did. There are some pictures of the forum. I'm building this reactor for commercial purposes. (Http://www.eco-promservice.ru/oborudovanie/fotovideo) looking at this site, I'm doing my own system. There are diagrams and pictures. Please look at them and tell me what you think. I do, there is a failure in the system, tell me. What are missing. The top of the oven, 1 and 2 will be like in the pictures.
    Thanks
    My only concern is that I think you are making the wrong choice of material for the Reactor Vessel. 304 is not the best for High Heat and especially in the presence of many Chemicals and Acids, most especially any Chlorides. This has been the issue with many Tyre reducing plants around the world, where Welds have cracked and oxygen has entered the vessel and huge explosions have resulted, with Deaths and major destruction.
    Last edited by wheels; 06-22-2014, 08:09 PM. Reason: Typing mistake

    Comment


    • Kedigen, nice work.

      Looking at the schematic drawing and relative sizes of the parts, I wondered if there is going to be enough reflux capability?

      Is there provision to divert the excess gas feed in times when the reactor is already at optimum temperature? Perhaps storing the gas to one side for later use?

      The second condenser inlet is near the bottom. I suppose you want the vapor to bubble through the condenser contents. Please be aware that the higher the level of condensed liquid, the more back pressure on the reactor.
      http://diydiesel.blogspot.co.nz/

      Comment


      • Originally posted by kedigen
        Thanks for the reply wheels
        First, even if cracks steam will come out. oxygen can not enter there. The durable steel 304 for this job. I tested with aluminum cookware, the top cover of the steam output gap. but it was not a problem. I tested the device later, when you open the plastic feeding the flames took place. the reactor, and the product. After a few months already, make a second reactor in the oven, I'm thinking of using exchange. for will be go out, be able to control. if it is older, we can change.
        I have to say, that is quite an effort of engineering. Well done.

        Keep this info for reference for when the Vessel needs to be replaced in the Future. I have worked with many Stainless Steel materials over the years, in all sorts of applications.
        304L and 316L have very similar chemistrys, except 316L withstands Chlorides better than 304L. But neither perform very well with high temperatures. They both significantly lose strength when heated and can easily distort and 316L suffers from embrittlement at high temperature's and will crack. Neither of them should be used in heat above 800DegC.
        There is a 304H that has a higher carbon content that 304L and will perform slightly better. The L stands for Low carbon SST. In the 300 series, 309 and 310 both withstand high heat of around 1000degC, but will suffer from scale eventually and 310 can become brittle and crack after time.
        Never use Martensitic and Precipitation hardened SST. They are Temperature hardened and will soften dramatically at temperatures over their hardening temperature. The same applies to Duplex SST's. These metals suffer from embrittlement at temperatures over 350DegC and will crack.

        The best choice of SST is the Ferritic 446 which has a 24% Chromium content and can work happily in temperatures of 1100DegC with no scaling issues.
        Another very good choice of SST is 2111HTC. That will also perform very well in very high heat conditions. It has a high nickel content and thus can be expensive.

        Be aware that what makes Stainless steel "stainless" is oxygen reacting with the Chromium. In high heats and especially in a furnace, there is very little Oxygen, so the ability to self protect is greatly reduced.
        Because of that, plain old Mild Steel will work almost as well a many of the SST metals and being significantly cheaper, it is sometimes easier or cheaper to make a vessel from Mild steel with the view that it is replaced when needed.

        Comment


        • Originally posted by kedigen
          Beyond Biodiesel
          before 2kg, 6 kg and 30 kg prototoip did. There are some pictures of the forum. I'm building this reactor for commercial purposes. (Http://www.eco-promservice.ru/oborudovanie/fotovideo) looking at this site, I'm doing my own system. There are diagrams and pictures. Please look at them and tell me what you think. I do, there is a failure in the system, tell me. What are missing. The top of the oven, 1 and 2 will be like in the pictures.
          Thanks
          Very impressive work, kedigen. Thanks for reporting it to us here. What are you planning on using for a seal?

          Your schematic suggests that the top of your reactor and the catalyst unit are not going to be insulated. If not, then I would expect that you will lose too much heat for cracking to take place, and/or your fluid stream will just reflux indefinitely.

          Your first device after the catalyst device is a heat exchanger. This could pose a serious plug problem with either coke or, if you are planning on cracking plastics, then uncracked plastics could plug it up.

          It would be better to have a vessel with the condenser above it, so that you have a secondary refluxing zone above the vessel, where condensates will collect, then drain back into the vessel.
          I have been running various blends of waste oils and unleaded gasoline in a 1983 Chevy G-20 van with a 6.2L diesel V-8 engine, with a Stanadyne Rotary DB2 IP since Feb, 2007. I have started the engine with no difficulty and no block heater on an 80/20 (WVO/gas) blend down to 0F (-18c). I have found that by blending as little as 15% gasoline in the summer, and as much as 50% in the winter, my engine starts and runs as if it was running on diesel fuel.

          Comment


          • Thanks, Wheels, for the writeup on stainless steel. I found it very useful.
            I have been running various blends of waste oils and unleaded gasoline in a 1983 Chevy G-20 van with a 6.2L diesel V-8 engine, with a Stanadyne Rotary DB2 IP since Feb, 2007. I have started the engine with no difficulty and no block heater on an 80/20 (WVO/gas) blend down to 0F (-18c). I have found that by blending as little as 15% gasoline in the summer, and as much as 50% in the winter, my engine starts and runs as if it was running on diesel fuel.

            Comment


            • Thanks, Wheels, for the writeup on stainless steel. I found it very useful.
              I have been running various blends of waste oils and unleaded gasoline in a 1983 Chevy G-20 van with a 6.2L diesel V-8 engine, with a Stanadyne Rotary DB2 IP since Feb, 2007. I have started the engine with no difficulty and no block heater on an 80/20 (WVO/gas) blend down to 0F (-18c). I have found that by blending as little as 15% gasoline in the summer, and as much as 50% in the winter, my engine starts and runs as if it was running on diesel fuel.

              Comment


              • Originally posted by Beyond Biodiesel View Post
                Thanks, Wheels, for the writeup on stainless steel. I found it very useful.
                You are welcome.
                I find it amusing when People talk about Grades of Stainless Steel in terms of Quality. For example, some think that 316 is a better grade to 304 because the Number is Higher. Or because 316 is better in Salt water, it must be a better quality. One very incorrect assumption that I come across often, is if a Stainless Steel is magnetic, it is therefore a low grade and cheaply made, which is not the case at all. Every Grade of Stainless steel is made for a specific range of use. Each has advantages and Disadvantages. There is no one grade better than all others, it comes down which grade is best for purpose.
                There are about 150 different grades of Stainless Steel.
                In fact the same can be said for any Metal and most especially any form of Alloyed Metal.

                Comment


                • Greetings guys, i'm improwing my retort insulation, and wanted to get your opinion on this. I want to put the reactor inside a barrel and fill the gap with insluation (much like Excalibur),pearlite is no option, but i have unlimited acces to clay, sand, ash, and glass. I was wondering if it is better to fill it up with just glass or just ash, or clay, or a mix between, all or some of them.
                  Thanks!

                  Comment


                  • retort

                    great work kedigen..keep it up and thanks for everyone you upload photos and help other....thanks beyond biodiesel and excalibur and wheels i find many help from them..thanks

                    Comment


                    • Originally posted by fox32 View Post
                      Greetings guys, i'm improwing my retort insulation, and wanted to get your opinion on this. I want to put the reactor inside a barrel and fill the gap with insluation (much like Excalibur),pearlite is no option, but i have unlimited acces to clay, sand, ash, and glass. I was wondering if it is better to fill it up with just glass or just ash, or clay, or a mix between, all or some of them.
                      Thanks!
                      Follow the advise we gave jonathan if you want to make some form of a solid cement insulation.
                      But I don't understand what you mean by filling the gap between retort and barrel. If you mean the gap between outer barrel and retort, that is the gap you need to allow heat to get up around the retort. You will want to have heat all around the retort, not just at the bottom. Plastic is a very good insulator and heat does not transfer through it very well, so heat all around is essential to ensure the melting takes place as fast as is possible.

                      Comment


                      • Yes,actually i have the heating through a pipe that goes through the reactor, working as a heat exchanger,the heat going from the inside out.I was refering at gap between the barrel surounding reactor and outer barrel. i don't need to make it like a cement, i was thinking to fill that gap, just pour it in there dry and pack it tightly. I will also have rockwool at exterior. Thanks!

                        Comment


                        • Fox32
                          If perlite isn't an option then how about vermiculite , expanded clay aggregate, or maybe pumice could be worth a try.
                          The expanded clay is used in the hydroponic industry. It looks interesting as its' full of air pockets, likewise for pumice.
                          I have used vermiculite, not the others..
                          http://diydiesel.blogspot.co.nz/

                          Comment


                          • Originally posted by fox32 View Post
                            Yes,actually i have the heating through a pipe that goes through the reactor, working as a heat exchanger,the heat going from the inside out.I was refering at gap between the barrel surounding reactor and outer barrel. i don't need to make it like a cement, i was thinking to fill that gap, just pour it in there dry and pack it tightly. I will also have rockwool at exterior. Thanks!
                            Filling the gap with dry, loose ash will work just fine for insulation. Coke is an even better insulator, but it will burn at 1200F (650c) unless O2 is not present.
                            I have been running various blends of waste oils and unleaded gasoline in a 1983 Chevy G-20 van with a 6.2L diesel V-8 engine, with a Stanadyne Rotary DB2 IP since Feb, 2007. I have started the engine with no difficulty and no block heater on an 80/20 (WVO/gas) blend down to 0F (-18c). I have found that by blending as little as 15% gasoline in the summer, and as much as 50% in the winter, my engine starts and runs as if it was running on diesel fuel.

                            Comment


                            • immersed heater

                              I have a question for all the PROs on this topic, regarding immersed heater element.

                              Just wanted to state I read most of this topic and I just couldnt find the answer. It has been brought up but discarded because immersed water heaters are not designed for high temperatures!

                              My question is for scenario of turning WMO to diesel...

                              Would it be safe to have an immersed heater element inside the main reactor where WMO is if said heater element IS designed for temperatures up to 1000 C or more?

                              Thanks

                              Comment


                              • Originally posted by osamaricu_te View Post
                                I have a question for all the PROs on this topic, regarding immersed heater element.

                                Just wanted to state I read most of this topic and I just couldnt find the answer. It has been brought up but discarded because immersed water heaters are not designed for high temperatures!

                                My question is for scenario of turning WMO to diesel...

                                Would it be safe to have an immersed heater element inside the main reactor where WMO is if said heater element IS designed for temperatures up to 1000 C or more?

                                Thanks
                                No it won't. You will end up with two problems and one difficulty. Firstly it will not withstand Acids and will corrode through the very thin protective jacket very quickly. Secondly, it is not designed to operate at the temperature you will need. Water will keep the element at 100degC (212degF) because it is an excellent liquid at drawing the heat away. But Oil is not so good at wicking away the heat and it has a lot of carbon in it that will cake to the element surface and serve to insulate the element and of course, you have to have a temperature 4x hotter than water boils at. The difficult part is the Seal at it's base will be very difficult to maintain sealed. It is possible, but difficult.
                                So all in all, it is not something that will last long term.
                                The idea is a good one though and one that I have been scratching my head on for some time. I think the way to do it is to have a center Pipe and the element is inside that pipe. But there needs to be something inside that pipe that transfers the heat from element to walls of pipe. I have thought about perhaps mounting the element in a Pipe and then filling the pipe/element with molten Aluminium. This would ensure a good conduction of heat to pipe wall. Aluminium has a melting point of 630 degC, so melting is not an issue.

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