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  • Originally posted by MangiPNG View Post
    Excalibur, I have studied your setup very closely and have started to build my system based around most of your principles and methods using the scraps I can find.
    I am wanting to use copper gaskets between every flange through the whole system. I have made all the flanges and lids out of 15mm MS/PLT myself using Oxy and a drill. The only flanges which are factory made are between the retort and reflux. The Retort is made from an old oxy cylinder and the reflux is from an old compressor cylinder. A few questions, does it matter if the reflux is larger in diameter and shorter in length then the retort? (I will be using a catalyst packed reflux same as yours) the length of the pipe from the reflux to the condenser is there a max or min I should be aware of? or does it depend on the gas temp entering the condenser?? My condenser is also bigger, the internal pipes are 40ID x 750 with a water jacket around them, thinking of packing them with glass? I want to incorporate a vacuum into the system for safety would the internals of an air conditioner or vacuum cleaner do? maybe if I fabricate the blades out of gauge sheet to replace the plastic to deal with the heat? Sorry for all the questions but I'd rather not kill myself trying.
    WMO is not quite so much of an issue re having to vacuum out the Air. But if you want to be sure, then a cheap air compressor works the best. Just connect the suck side instead of the pressure side. A Vacuum cleaner would not suck hard enough. I am not sure what part you mean re the Air Conditioner. But the Refrigeration pump can be used, although it would be slow. Once again, you need to connect the suction side. Leave a little oil in it, but not too much or it will blow the oil out everywhere.

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    • Originally posted by MangiPNG View Post
      Thanks for the response guys.. I can't tell you how much of a motivation it is just to get a reply.

      Wheels I plan to start off with WMO as I currently have about 12,000L which I can get for FREE monthly from a local transport company who wants to get rid of it. I don't plan to use copper anywhere else in my system only as gaskets, I think I read here or somewhere that copper accelerates the oxidation of the fuel?? so I'm thinking the less I use the better.
      Try a run without the catalyst first. WMO does not need a great deal of cracking. Temperature will have a big influence on cracking and it might be best to see what you get first. What the output product you get will depend on what the waste is made up from. As in, has it had fuels thrown in, cleaners/solvents, Gear oils, transmission oils and so on. So not everyones WMO supply will be the same. Also you are likely to find a great deal of water that will settle to the bottom of the drum. It is good to remove as much as possible before you add it to the retort.

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      • Originally posted by chacowako View Post
        Hi guys im stuck at a problem I cant find a way to check the fluid level of my reactor.
        Ive checked probes on the internet i can only find rated up to 200c for 450c Im having a hard time I found 1 that can reach 900c but costs $1000 !!! Way over my budget.
        any genius got a solution? I would be very grateful
        also i read on previous posts that an o2 sensor is used? Ive read on internet I have no idea how it should work.
        ultra sonic level sensors are available with many automation companies but it is too risky to get the retort open in middle of process possibility of explosion is there I fairly suggest if you want your process to be continuous you have to opt for horizontal reactor vessel instead of verticle
        Last edited by sunilkm153; 10-10-2014, 06:33 PM.

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        • Originally posted by wheels View Post
          What the output product you get will depend on what the waste is made up from.
          Actually to add to that, excalibur and I have been discussing an issue we have both had when running with WMO. We get a varnish or gum that makes the heavier fractions very dark in color and the lighter fractions more Amber. It does not want to filter out. But once in the Vehicle fuel system, it will coat Filters and other metal part in this brown colored resin material. So a need for purifying the Fuel better, needs to be considered. Because WMO is not what I will normally be producing, it has not bee a priority for me to look into. Excalibur has been trying various methods and I am sure he will come up with some kind of cure eventually. But if anyone else has been able to remedy thos problem, without going the expense and difficulty of huge complex Filtration, like clay or ceramic, then please let us know.

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          • gasket problem

            my answer for the retort opening gasket is to make a male and female steel ring flange.The female bottom flange is cut 20mm deep with a 10mm round groove machined through center.The male top flange is also 20mm thick with a 10mm vertical groove protruding.All grooves are square.There are 8 threaded bolt holders spread around the plates.The female groove is then filled with graphite 10mm rope for machine gaskets available from Bearing Man.The lid is bolted together and never failed.Cost of the system approx 150 dollars.Built four units like this and no failure when constant opening and closing.
            Last edited by rozier56; 10-11-2014, 05:48 AM. Reason: correction

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            • waxing

              i have a system that seems to produce a lot of wax right up to reflux temp of 330*c.Has anybody else had this happen when using plastic raws?What temp does this wax start at and do i need to run at higher temp?

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              • Originally posted by rozier56 View Post
                i have a system that seems to produce a lot of wax right up to reflux temp of 330*c.Has anybody else had this happen when using plastic raws?What temp does this wax start at and do i need to run at higher temp?
                Wax is a hydrocarbon in the Paraffin range and what many Plastics are made from. So when it is vaporized again, the Plastic reverts back to what it was made from and you get Paraffin. In many respects, it means you have a very good process taking place re the melting. But the pyrolysis is just one part of a very complex chain or processes. It is essential to understand the entire process.
                So firstly, the plastic is melted to the point where it vaporizes. The Vapors/Gasses are the various Hydrocarbon chains that originally went into making the Plastic. That part is Pyrolysis. Pyro meaning heat and Lysis, meaning to break apart.
                These individual chains may need to be broken in to shorter chains. That part of the process is called "cracking', or "fractionating". It is the most complex part of the entire process. You have to know just what chain length is mainly being produced and then adjusting the process to produce the type of chain you mostly want. This part will vary for everyone. There is no fixed Golden rule, because the formation of a Hydrocarbon length is determined by the Type of plastic, the temperature the melt is performed at, the size and shape of the vessel and pipe work etc, which will all alter the time the chain is in the heating zones for. Then there is size and shape of catalyst container, if catalyst is being used at all and what catalyst is being used. So there are just too many variables to say that if if you do a certain thing, you will get a certain result.
                So in answer to your question, Wax equals long chain lengths. They have to be broken to produce shorter chain lengths. Just how that is done is by adjusting one or maybe all of the following things like Retort temperature. Using a Catalyst(which will vary on quantity of catalyst used and operating temperature).
                And finally, the distillation process. If you have a slightly more complex, but tightly temperature controlled multi pot Distillation process, then you should be able to distill the heavy Hydrocarbons(waxes) in the first pot, the mid range(diesel weight) in the second pot and the very light fractions(petrol weights) in the third.

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                • Excalibur, can you check your email please.thks.

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                  • Originally posted by rozier56 View Post
                    Excalibur, can you check your email please.thks.
                    Just in case you have not heard from Excalibur, he is currently traveling and may or may not get this message of yours, but will be back home in a few days.

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                    • Thks ,Wheels for info and your reply to question.

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                      • Originally posted by wheels View Post
                        WMO is not quite so much of an issue re having to vacuum out the Air. But if you want to be sure, then a cheap air compressor works the best. Just connect the suck side instead of the pressure side. A Vacuum cleaner would not suck hard enough. I am not sure what part you mean re the Air Conditioner. But the Refrigeration pump can be used, although it would be slow. Once again, you need to connect the suction side. Leave a little oil in it, but not too much or it will blow the oil out everywhere.
                        I think I will get an air compressor as you say. What type of pressure pressure is needed? I don't want to end up sucking all the WMO out of the retort. The main products I am after is Diesel.

                        Comment


                        • Originally posted by rozier56 View Post
                          my answer for the retort opening gasket is to make a male and female steel ring flange.The female bottom flange is cut 20mm deep with a 10mm round groove machined through center.The male top flange is also 20mm thick with a 10mm vertical groove protruding.All grooves are square.There are 8 threaded bolt holders spread around the plates.The female groove is then filled with graphite 10mm rope for machine gaskets available from Bearing Man.The lid is bolted together and never failed.Cost of the system approx 150 dollars.Built four units like this and no failure when constant opening and closing.
                          My problem with the setup you describe is, most of the materials are very difficult to source locally and going to a machinist cost an arm an a leg here. Plus I am trying to build everything from scraps with minimum cost, except for the precision instruments like for controlling temp and pressure etc.. But always keeping the safety aspect 100% in mind.

                          Comment


                          • Originally posted by MangiPNG View Post
                            I think I will get an air compressor as you say. What type of pressure pressure is needed? I don't want to end up sucking all the WMO out of the retort. The main products I am after is Diesel.
                            Don't worry about sucking out too much. Providing you have a solid containment vessel and everything is Air tight, the a maximum vacuum can be pulled and the Oil will stay put in the bottom of the vessel. The more air you can pull out, the better and safer everything will be. One really big plus with having a good vacuum is that you lower the boiling point of everything. That will not be of concern with the Oil as the pressure should be neutral by the time the Oil gets up to temperature. But it will aid in removal of water at a much lower and earlier temperature. It would be helpful to have a Vacuum gauge of course and basically vacuum the Air out, then watch the gauge and when it has returned to zero, you can open the valve to allow the Gas to flow. Remember to close the Valve when vacuuming, or you will suck all your Bubbling water back through the system and maybe into the Compressor Pump.
                            One wee tip, reduce the oil level in the compressor pump a little. Not essential, but when you use it as a vacuum pump, it can pick up some of that oil and blow it out the outlet. It shouldn't do any damage, just annoying.

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                            • Originally posted by MangiPNG View Post
                              My problem with the setup you describe is, most of the materials are very difficult to source locally and going to a machinist cost an arm an a leg here. Plus I am trying to build everything from scraps with minimum cost, except for the precision instruments like for controlling temp and pressure etc.. But always keeping the safety aspect 100% in mind.
                              Яндекс.Фотки

                              go through this album, hopefully it will help
                              Last edited by torak; 10-13-2014, 09:49 AM.

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                              • Originally posted by rozier56 View Post
                                my answer for the retort opening gasket is to make a male and female steel ring flange.The female bottom flange is cut 20mm deep with a 10mm round groove machined through center.The male top flange is also 20mm thick with a 10mm vertical groove protruding.All grooves are square.There are 8 threaded bolt holders spread around the plates.The female groove is then filled with graphite 10mm rope for machine gaskets available from Bearing Man.The lid is bolted together and never failed.Cost of the system approx 150 dollars.Built four units like this and no failure when constant opening and closing.
                                Hi can you post pictures please or send me pictures thanks!!

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